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Using Microscopes for Macro Savings

Closing Data Gaps: Utilizing Field Microscopy for Real-Time CCR Identification

The accurate identification and delineation of coal combustion residuals (CCR) in complex subsurface environments present significant logistical and financial challenges, particularly when distinguishing ash from native soils and sediment or historical fill. Traditional characterization methods rely on visual field observations followed by a 7- to 10-day turnaround for polarized light microscopy analysis. Those methods often result in inaccurate horizontal and vertical delineations, which can lead to costly remobilization activities. These challenges are amplified in high-cost environments, such as drilling where barges, cranes, and other high-cost standby equipment is required.

SynTerra conducted a successful pilot test at an industrial cooling pond adjacent to a CCR ash basin, where historical records indicated potential ash migration of unknown extent. To overcome the limitations of the “Sample → Ship → Wait” workflow, SynTerra implemented a novel portable field microscopy protocol to identify the signatures of CCR. By leveraging the unique morphology of cenospheres (hollow, glassy spheres formed under high-temperature combustion that serve as a “smoking gun” for CCR), field geologists were able to make definitive “yes or no” determinations within 15 minutes of sample recovery.

The real-time data collected and evaluated by this methodology allowed for immediate adjustments to the sampling plan including the repositioning of the drilling barge to new coordinates, drastically reducing mobilization costs and standby time for specialized, expensive equipment. This approach is also being used to directly address data gaps essential for CCR Legacy Rule Facility Evaluation Reports by quickly providing defensible spatial data on ash presence. The integration of field microscopy with traditional soil classification-based logging aids data-driven decisions that align with evolving regulatory requirements.